For many years
I was just a hobbyist brewer, and in fact, I was making spirits
of my own since I was 12 years old (under adult supervision:-).
Everything was so exciting, and everyone was happy about the
results. As time went by, I started to ask myself some
questions, like why my homebrew was not that good and tasted
more like rocket fuel, so I began to think of how to improve the
quality of my brew.
TThe
reality is: that new technologies of distillation and
purification exist and are widely used by leading alcoholic
beverage producers. And this new approach to distillation is
evident because, along with our smelly homebrewed liquors,
we have exceptional products on the shelves of our local
liquor shops.Moreover,
the cost of good liquor production is twice as cheap as the
average cost of homebrew production per unit! I know it is
because I was co-owner of a vodka factory, and the rule of
business is - to spend less and make a more significant
margin plus keep quality high.
But the big guys do not want people like you to know how to
make authentic, high-quality alcoholic beverages because
they can lose their market, but as long as simple people
make simple homebrew, the same people will buy quality
liquor despite their hobby again and again. While in the
vodka business, I was personally suppressing any information
about our equipment and the production methods.
As the basis for spirit production, I adopted the method
used in Russia to produce high-quality spirits by leading
vodka companies; the alcohol is made in two stages.
The first stage is the production of raw or crude alcohol -
where the main goal is to separate alcohol from the mash and
all by-products that naturally occur in any ferment: acids,
salts (yeast nutrition), and mechanical particles.
The second stage is actual fractioning (rectification),
where the raw, crude alcohol that contains esters, methanol,
ethanol (alcohol we are aiming at), and smelling butyl
alcohol is redistilled in a fractional column.
The construction of a fractional
(reflux) column makes it possible for the alcohol to be
re-distilled inside the column more than 30 times before it
reaches the collection vessel ( this ability of the column
gives us the strength of the alcohol of 95 - 96% alc/vol).
The correctly built fractional column creates some
fractions' queue inside the column where the lightest spirit
fraction is located at the top and gets collected while the
heaviest alcohol fraction is yet situated at the bottom. The
next in the queue, and heavier one, is replacing the lighter
one, and so on (this ability of the column gives us the high
quality of alcohol because one can separate and collect all
fractions one after another very precisely.
The understanding of amounts of different
fractions in the crude alcohol plus the measurement of total
spirit percentage in the batch before fractioning makes it
possible to forecast the whole distillation process. These
include the time of distillation, amounts of different
fractions in liters or milliliters, and percentages
concerning total alcohol amount.
Thus, instead of relying on carbons (people still think that
carbon filtration will eliminate all the impurities from the
final product), one can separate all contaminants from each
other with a fractional column during distillation, and all
you need to do; is to dilute your distilled spirit with
water and filter only if you wish so.
The 25L fractional homebrew
still has all you need to perform precise distillation; it
has one small column for raw spirit production and a big
fractional column for high-quality food-grade alcohol production.
The small column can also be used along with an infuser or
by itself for aromatic beverage production, where you can
distill alcohols soaked with herbs or fruits ( I use the
small column to make absinthe).
When the crude alcohol is ready for fractional
distillation, all data about spirit percentage and amount is
taken. It is mixed with water, which helps to bound heavy
fractions and odors, then loaded into the still and
fractionally distilled. The result - is high-quality ethanol
for further beverage production.
The whole still arrangement, which includes two columns, is
designed to produce high-quality ethanol at the highest
possible percentage. There are two columns: the first is
intended to deliver a low-quality spirit from the fermented
wash (mash, beer, wine) and works as a pure pot still. The
primary purpose of this column is to separate alcohol from
the wash.
The
second (fractional) reflux column (which has the option of
manual reflux ratio control that does not depends on cooling
water flow speed or temperature) is designed to fractionally
separate all the impurities from the low-quality spirit
after the first distillation.
The fractional column is used only for crude alcohol - or
moonshine quality redistilling and separates all impurities
physically from alcohol.
Thus with the help of a fractional column, you can get all
fractions precisely defined. During distillation, you will
rely on a mathematical calculation of spirits amounts based
on fractions percentage calculation - this means that you
will know how much of each bit you will get even before
starting your distillation.
Suppose you are familiar with some reflux columns. In that
case, all reflux columns are capable only of producing the
alcohol with the relatively high percentage of alcohol in
the ethyl/water mix and not capable of separating any
impurities—the portion of the alcohol drops during the
distillation. The ratio and the quality of alcohol are
achieved and controlled by the speed of cooling water flow -
believe me, it is almost impossible to accomplish any good
quality results with this type of distillation system.
You will get out of simple reflux type of still just what
it can give you.
The distillation system described on this page is a real
fractional distiller where one can control reflux ratio and
spirit speed flow regardless of water flow rate. The alcohol
collection/flow control valve can be closed completely. The
column will utilize all distillate back into the column's
internal space, and no pressure build-up will ever happen.
All fractions get separated according to their physical
properties. This fractional distiller will give you the
maximum possible percentage of alcohol: 95%+ from the
beginning of distillation to the end. All separated
impurities can be used to power four-stroke engines (I use
them for my lawnmower).
Just a few words about
filtration: some people believe activated carbon can absorb
impurities such as methanol (heads), but this is not right.
One can run the bottle of methanol through the activated
carbon filter and get the same poisonous methanol from the
other end of the filter, and it will be sparkling clean, but
there. If activated carbon's pores are big enough for the
water to run through, they are even more prominent for
anything more liquid than water. All the carbon does is
absorb the odors and mechanical particles (cloudiness). I
prefer the activated carbon from coconut shells over the
carbon produced out of peat.
Never filter undiluted alcohol, the carbon works only up to
60% spirits strength, it is simple - the water that is added
to the alcohol during dilution is bounding up with some
impurities, and the carbon keeps this bounded up molecules.
Undiluted spirit will just run through the carbon.
Here is some facts:
Here is are some facts to Save your $$$ on distillation!!!
The fractional distillation offers low cost of distillation (under NZ $4 per
litre of 40% vodka) and highest quality possible.
Here is some example:
To make 5L of 40 % vodka you will need: Sugar – 6kg = $7.20 Super yeast – one pack = $9.00 Power - $0.20 per unit, total 9kw =$1.80
All this will give you >=2L of 96% spirit that after dilution with water makes 5L of vodka.
Total cost = $18.00 divided by 5L = $3.6 per
litre of high quality 40% alcohol, just try to find the distillation system that will offer high quality and yet low production cost. The prices in your country may be different from above.
The 25L still is now available for international
customers. Stills are build to your order and delivered by
air post within ten business days,
The fractional distiller can also be used and ordered as a
water purifier and essential oils extractor, the still can
be used for a small scale fuel ethanol production. Buy the "Alex 25" still construction plans, parts and stills: